PAL INSTRUMENTATION  (Detailed Listing)

 

Molecular Characterization:

 

         THF-GPC-MALS

o   FLO-M Vacuum degasser

o   Agilent 1100 Pump

o   Agilent 1100 autosampler

o   Wyatt Dawn-EOS LS Detector

o   Agilent 1200 DRI detector

 

         Aqueous-GPC-MALS

o   FLO-M Vacuum degasser

o   Isco Syringe Pumps (500mL)

o   Manual Injector

o   Wyatt Dawn-DSP LS Detector

o   Waters 410 DRI Detector

 

         Toluene-GPC-MALS

o   FLO-M Vacuum degasser

o   2 Isco Syringe Pumps (500mL)

o   Manual Injector

o   Wyatt Dawn-EOS LS Detector

o   Hitachi DRI detector      

 

         Mixed GPC (aqueous or Organic)

o   FLO-M Vacuum degasser

o   2 Isco Syringe Pumps (500mL)

o   Manual Injector

o   Viscotek Viscosity detector

o   Waters 410 DRI Detector

 

         Viscotek TDA-302 Triple detector

 

         Asymmetric Flow Field Flow Fractionation (AF4) (can be used as GPC)

o   Wyatt Eclipse 2 (Organic and Aqueous capability)

o   FLO-M Vacuum degasser

o   Agilent 1100 Pump

o   Agilent 1100 autosampler

o   Wyatt Heleos LS detector with DLS Capability and Temp. Control (0 to 60C)

o   Wyatt rEX DRI detector

o   Wyatt Viscostar viscosity detector

 

 

Thermal Analysis

 

         TA 2920 Modulated Differential Scanning Calorimeter (DSC) with Refrigerated System Cooling (RSC)

 

         TA 2920 Modulated Differential Scanning Calorimeter (DSC) with Liquid Nitrogen Cooling

 

         TA 2920 High Pressure Differential Scanning Calorimeter (DSC)

 

         TA 2950 Modulated High Sensitivity Thermogravimetric Analyzer (TGA)

 

         TA 2970 Dielectric Thermal Analysis (DEA)

 

         TA Q800 Dynamic Mechanical Analyzer (DMA) with:

o   NPC (Nitrogen Purge Cooling)

o   Compression clamp

o   Submersion compression clamp

o   Dual surface film clamp

o   Single/dual Cantilever Clamp

 

 

Scattering

 

         Malvern Zetasizer Nano ZS with Titrator

o   One angle Backscattering (173)

o   Zeta Potential

o   Titrator

 

         Multiangle Dynamic/Static Light Scattering System

o   Crystal Laser CL-2000 Diode Pumped Laser (532nm, 500mW)

o   Melles Griot He-Ne Laser (632.8nm, 15mW)

o   Coherent Innova 90 Ion Laser (488, 514.5, 657 nm, 500mW)

o   Oriel 77341 PMT

o   EMI 9863 PMT

o   Pacific Industries AD-126 Amplifier Discriminator and 126 Lab Photometer

o   ALV Correlator

o   Neslab RTE 111 Circulating Bath

 

         Thorn EMI Photon Counting System ( Not in Use)

 

         Beckman Coulter LS-200 Laser Diffraction Particle Size Analyzer

o   Micro Cell Accessory

o   Dry Powder sampler

o   Standard Flow sampler

 

 

 

Microscopy

 

         Olympus BH Polarized Optical Microscope (POM).

o   AmScope MD1900 Digital Camera

 

         Olympus BX50 Microscope

o   Mettler FP82 Hot Stage

o   Mettler FP80 Central Processing unit

o   Mettler Photodetector

 

         Leitz Metallux 3 Fluorescence Microscope.

o   MTI SIT 66 CCD Camera

 

Balances

 

         Sartorius A 120 S Analytical Balance (4 decimal)

         Sartorius A160 P Analytical Balance  (5 decimal)

         Cahn C-31 Microbalance (6 decimal)

 

 

Other Instruments/ Capabilities

 

         Barnstead Nanopure Water System

o   With Ultrafilter (0.005m)

 

         Perkin Elmer LS50B Luminescence Spectrometer

o   Temperature Control (VWR 1167 Circulating Bath)

 

         Agilent 8453 DAD Spectrophotometer

o   7 Multicell Accessory

o   Temperature Control (VWR 1167 Circulating Bath)

 

         Thermo Orion 420 pH Meter

 

         Beckman Microfuge E Micro Centrifuge

 

         IEC Clinical centrifuge

 

         American Scientific BT-23 Thermostated Shaking Bath

 

         Fisher Isotemp Oven (up to ~ 200C)

 

         National Appliance Company 5831 Vacuum Oven (up to ~ 200C)

o   Welch Duo-Seal Vacuum pump, Trap

 

         VWR Vacuum Oven (up to ~ 200C) (Not in Use)

 

         Sonic VibraCell VC-750 Sonicator

o   Several Probes

o   Sound Proof Cabinet

 

         Branson 2210 Sonicator

 

         Solvent Filtering Station

o   1L Organic Flask

o   1L Aqueous Flask

o   GAST Diaphragm Pump

 

         Buchi RE-121 Rotovap

o   Buchi B-480 Water Bath

o   Neslab RTE-110 Cooling Circulator

 

         NIMA Langmuir Blodgett trough ((Not in use)

 

         HP 5890 Series II GC  (Not in use)

o   FID

o   ECD

o   Antek 705D Nitrogen Detector

 

         HP 1090 HPLC (Not in use)

o   DAD Detector

o   ESA Coulochem Electrochemical Detector

 

 

Other Instruments (NOT PAL)

 

         Bruker EMX 10/2.7 Electron Paramagnetic Resonance (EPR) spectrometer

o   10 magnet

o   2.7 kV power supply

o   Microwave X band solid state bridge

o   microwave frequency counter

o   ER 4119HS high sensitivity Resonator

o   ER 4105DR double resonator

o   Aquax aqueous solution cell accessory

o   Liquid nitrogen Cryostat (Not in use)

 

         OLIS-RSM-1000 RSM Stopped Flow

o   Temperature Control (VWR 1167 Circulating Bath)

 

         TSI Differential Mobility Analyzer (DMA)

o   Aerosol Generator

o   3076 Constant Output Atomizer

o   3074B Filtered Air Supply With HEPA filters

o   Lindberg/ BlueM Tube Furnace (up to 1100C)

o   3080 Electrostatic Classifier (2)

o   308100 Classifier (2)

o   308500 Classifier

o   3776 Ultrafine Condensation Particle Counter

 

 

MS Word Version of PAL Instrumentation

 

PAL_BOILERPLATE_022618 .doc

 

Last Edited 04/13/2018

 

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