PAL INSTRUMENTATION (Detailed Listing) (110922)
Molecular Characterization:
· THF-GPC-MALS
o FLO-M Vacuum degasser
o Agilent 1100 Pump
o Agilent 1100 autosampler
o Wyatt Dawn-EOS LS Detector
o Waters 410 DRI Detector
· Aqueous-GPC-MALS
o FLO-M Vacuum degasser
o Isco Syringe Pumps (500mL)
o Manual Injector
o Wyatt Dawn-DSP LS Detector
o Waters 410 DRI Detector
· Toluene-GPC-MALS
o FLO-M Vacuum degasser
o 2 Isco Syringe Pumps (500mL)
o Manual Injector
o Wyatt Dawn-EOS LS Detector
o Hitachi DRI detector
·
· Tosoh EcoSEC Elite HLC-8420GPC with Lens3 Light Scattering Detector
o Vacuum degasser
o Pump
o autosampler
o Lens3 LS Detector
o DRI Detector
· Viscotek TDA-302 Triple detector
· Mixed GPC (aqueous or Organic)
o FLO-M Vacuum degasser
o Agilent 1100 Pump
o Agilent 1100 autosampler
o Wyatt Heleos LS detector with DLS Capability and Temp. Control (0 to 60C)
o Agilent 1200 DRI detector
Thermal Analysis
·
TA Discovery DSC250 Modulated Differential Scanning Calorimeter (DSC) with Refrigerated System Cooling (RSC-90) -90C to 550C
TA Q100 Modulated Differential Scanning Calorimeter (DSC) with Refrigerated System Cooling (RSC-40) -40C to 400C, or Liquid Nitrogen Cooling
TA Discovery TGA550 Modulated High Sensitivity Thermogravimetric Analyzer (TGA)
· TA Q800 Dynamic Mechanical Analyzer (DMA) with:
o NPC (Nitrogen Purge Cooling)
o Compression clamp
o Submersion compression clamp
o Dual surface film clamp
o Single/dual Cantilever Clamp
TA Discovery HR 20 Advanced Hybrid Rheometer
Environmental Testing Chamber (ETC) (-55oC to 600oC)
Upper and Lower Peltier Plates (-40oC to 200oC)
UV Curing Accessory
TA Ares Advanced Rheometer AR200 with ETC (Environmental Testing Chamber), Tension and Asphalt Geometries
Scattering
· Malvern Zetasizer Nano ZS with Titrator
o One angle Backscattering (173)
o Zeta Potential
o Titrator
· Multiangle Dynamic/Static Light Scattering System
o Crystal Laser CL-2000 Diode Pumped Laser (532nm, 500mW)
o Melles Griot He-Ne Laser (632.8nm, 15mW)
o Coherent Innova 90 Ion Laser (488, 514.5, 657 nm, 500mW)
o Oriel 77341 PMT
o EMI 9863 PMT
o Pacific Industries AD-126 Amplifier Discriminator and 126 Lab Photometer
o ALV Correlator
o Neslab RTE 111 Circulating Bath
· Thorn EMI Photon Counting System ( Not in Use)
· Beckman Coulter LS-200 Laser Diffraction Particle Size Analyzer
o Micro Cell Accessory
o Dry Powder sampler
o Standard Flow sampler
Microscopy
· Olympus BH Polarized Optical Microscope (POM).
o AmScope MD1900 Digital Camera
· Olympus BX50 Microscope
o Mettler FP82 Hot Stage
o Mettler FP80 Central Processing unit
o Mettler Photodetector
·
Balances
· Sartorius A 120 S Analytical Balance (4 decimal)
· Cahn C-31 Microbalance (6 decimal)
Other Instruments/ Capabilities
· Barnstead Nanopure Water System
o With Ultrafilter (0.005µm)
· Perkin Elmer LS50B Luminescence Spectrometer
o Temperature Control (VWR 1167 Circulating Bath)
· Agilent 8453 DAD Spectrophotometer
o 7 Multicell Accessory
o Temperature Control (VWR 1167 Circulating Bath)
· Thermo Orion 420 pH Meter
· Beckman Microfuge E Micro Centrifuge
· IEC Clinical centrifuge
· American Scientific BT-23 Thermostated Shaking Bath
· Fisher Isotemp Oven (up to ~ 200C)
· National Appliance Company 5831 Vacuum Oven (up to ~ 200C)
o Welch Duo-Seal Vacuum pump, Trap
· VWR Vacuum Oven (up to ~ 200C) (Not in Use)
· Sonic VibraCell VC-750 Sonicator
o Several Probes
o Sound Proof Cabinet
· Branson 2210 Sonicator
· Solvent Filtering Station
o 1L Organic Flask
o 1L Aqueous Flask
o GAST Diaphragm Pump
· Buchi RE-121 Rotovap
o Buchi B-480 Water Bath
o Neslab RTE-110 Cooling Circulator
· NIMA Langmuir Blodgett trough ((Not in use)
·
Other Instruments (NOT PAL)
· Bruker EMX 10/2.7 Electron Paramagnetic Resonance (EPR) spectrometer
o 10” magnet
o 2.7 kV power supply
o Microwave X band solid state bridge
o microwave frequency counter
o ER 4119HS high sensitivity Resonator
o ER 4105DR double resonator
o Aquax aqueous solution cell accessory
o Liquid nitrogen Cryostat (Not in use)
· OLIS-RSM-1000 RSM Stopped Flow
o Temperature Control (VWR 1167 Circulating Bath)
·
MS Word Version of PAL Instrumentation
Last Edited 11/09/2022