PAL INSTRUMENTATION  (Detailed Listing) (110922)

 

Molecular Characterization:

 

         THF-GPC-MALS

o   FLO-M Vacuum degasser

o   Agilent 1100 Pump

o   Agilent 1100 autosampler

o   Wyatt Dawn-EOS LS Detector

o   Waters 410 DRI Detector

 

         Aqueous-GPC-MALS

o   FLO-M Vacuum degasser

o   Isco Syringe Pumps (500mL)

o   Manual Injector

o   Wyatt Dawn-DSP LS Detector

o   Waters 410 DRI Detector

 

 

         Toluene-GPC-MALS

o   FLO-M Vacuum degasser

o   2 Isco Syringe Pumps (500mL)

o   Manual Injector

o   Wyatt Dawn-EOS LS Detector

o   Hitachi DRI detector      

 

     

         Tosoh EcoSEC Elite HLC-8420GPC with Lens3 Light Scattering Detector

o   Vacuum degasser

o   Pump

o   autosampler

o   Lens3 LS Detector

o    DRI Detector

 

  

         Viscotek TDA-302 Triple detector

 

         Mixed GPC (aqueous or Organic)

o   FLO-M Vacuum degasser

o   Agilent 1100 Pump

o   Agilent 1100 autosampler

o   Wyatt Heleos LS detector with DLS Capability and Temp. Control (0 to 60C)

o      Agilent 1200 DRI detector

 

 

 

 

Thermal Analysis

 

        

TA Discovery DSC250 Modulated Differential Scanning Calorimeter (DSC) with Refrigerated System Cooling (RSC-90) -90C to 550C

 

TA Q100 Modulated Differential Scanning Calorimeter (DSC) with Refrigerated System Cooling (RSC-40) -40C to 400C, or Liquid Nitrogen Cooling

 

TA Discovery TGA550 Modulated High Sensitivity Thermogravimetric Analyzer (TGA)

 

 

         TA Q800 Dynamic Mechanical Analyzer (DMA) with:

o   NPC (Nitrogen Purge Cooling)

o   Compression clamp

o   Submersion compression clamp

o   Dual surface film clamp

o   Single/dual Cantilever Clamp

        TA Discovery HR 20 Advanced Hybrid Rheometer

 TA Ares Advanced Rheometer AR200 with ETC (Environmental Testing Chamber), Tension and Asphalt Geometries

 

 

Scattering

 

         Malvern Zetasizer Nano ZS with Titrator

o   One angle Backscattering (173)

o   Zeta Potential

o   Titrator

 

         Multiangle Dynamic/Static Light Scattering System

o   Crystal Laser CL-2000 Diode Pumped Laser (532nm, 500mW)

o   Melles Griot He-Ne Laser (632.8nm, 15mW)

o   Coherent Innova 90 Ion Laser (488, 514.5, 657 nm, 500mW)

o   Oriel 77341 PMT

o   EMI 9863 PMT

o   Pacific Industries AD-126 Amplifier Discriminator and 126 Lab Photometer

o   ALV Correlator

o   Neslab RTE 111 Circulating Bath

 

         Thorn EMI Photon Counting System ( Not in Use)

 

         Beckman Coulter LS-200 Laser Diffraction Particle Size Analyzer

o   Micro Cell Accessory

o   Dry Powder sampler

o   Standard Flow sampler

 

 

 

Microscopy

 

         Olympus BH Polarized Optical Microscope (POM).

o   AmScope MD1900 Digital Camera

 

         Olympus BX50 Microscope

o   Mettler FP82 Hot Stage

o   Mettler FP80 Central Processing unit

o   Mettler Photodetector

 

       

Balances

 

         Sartorius A 120 S Analytical Balance (4 decimal)

         Cahn C-31 Microbalance (6 decimal)

 

 

Other Instruments/ Capabilities

 

         Barnstead Nanopure Water System

o   With Ultrafilter (0.005m)

 

         Perkin Elmer LS50B Luminescence Spectrometer

o   Temperature Control (VWR 1167 Circulating Bath)

 

         Agilent 8453 DAD Spectrophotometer

o   7 Multicell Accessory

o   Temperature Control (VWR 1167 Circulating Bath)

 

         Thermo Orion 420 pH Meter

 

         Beckman Microfuge E Micro Centrifuge

 

         IEC Clinical centrifuge

 

         American Scientific BT-23 Thermostated Shaking Bath

 

         Fisher Isotemp Oven (up to ~ 200C)

 

         National Appliance Company 5831 Vacuum Oven (up to ~ 200C)

o   Welch Duo-Seal Vacuum pump, Trap

 

         VWR Vacuum Oven (up to ~ 200C) (Not in Use)

 

         Sonic VibraCell VC-750 Sonicator

o   Several Probes

o   Sound Proof Cabinet

 

         Branson 2210 Sonicator

 

         Solvent Filtering Station

o   1L Organic Flask

o   1L Aqueous Flask

o   GAST Diaphragm Pump

 

         Buchi RE-121 Rotovap

o   Buchi B-480 Water Bath

o   Neslab RTE-110 Cooling Circulator

 

         NIMA Langmuir Blodgett trough ((Not in use)

 

     

 

Other Instruments (NOT PAL)

 

         Bruker EMX 10/2.7 Electron Paramagnetic Resonance (EPR) spectrometer

o   10 magnet

o   2.7 kV power supply

o   Microwave X band solid state bridge

o   microwave frequency counter

o   ER 4119HS high sensitivity Resonator

o   ER 4105DR double resonator

o   Aquax aqueous solution cell accessory

o   Liquid nitrogen Cryostat (Not in use)

 

         OLIS-RSM-1000 RSM Stopped Flow

o   Temperature Control (VWR 1167 Circulating Bath)

 

      

 

MS Word Version of PAL Instrumentation

 

PAL_BOILERPLATE_110922 .doc

 

Last Edited 11/09/2022

 

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