How To Guides |
THESE GUIDES describe techniques and use of the equipment in the Polymer Analysis Laboratory. A "mirror" (modified) copy is kept in the Applied Polymer Technology Extension Consortium (APTEC) website.
LSU Office of Environmental Health and Safety (EHS)
Request for Hazardous Material Pickup & Disposal (Through the EHS Assistant Home Page)
Chemical Inventory Management System (Through the EHS Assistant Home Page)
Safety Data Sheets (SDS) LSU Web Page
Millipore Sigma (Sigma Aldrich) (Enter product name in Product search box; Click on product; under documentation select SDS).
Excel Tricks
Solver Template (does a linear fit the nonlinear way)(.xlsx)
Solver Demo (fits sum of sine & cosine)(.xls)
Laboratory Notebooks (.ppt) (how to keep a decent lab notebook--more than you think)
Survival Skills (.doc) (how to graph, program, keep records, identify resistors, and other useful stuff)
Writing (advice from the macromolecular faculty)
Data Handling (.ppt)
Manuals: Link to user manuals of instruments/equipment in PAL (Password Protected)
Making Solutions (.doc)
Densitometry using the Paar DMA 58(.doc)
Differential Refractive Index (dn/dc)(.doc)
Excel Spreadsheet Template(.xls)
Brice-Phoenix Manual (.pdf)
Brice-Phoenix appendix (.pdf)
dn/dc Tutorial (from APTEC) (.pptx)
dn/dc tables and papers (Password Protected)
Abbe Zeiss refractometer (.pdf)
Nano Measurement Protocols (NIST)
Sample Preparation Protocols (NIST)
List of BOOKS Related to Light Scattering
Multiple-angle, multiple-correlator DLS (MADLS) (.doc)
Guinier Plot (Radius of Gyration from Light Scattering) (.doc)
Dynamic Light Scattering Minicourse (.pdf)
*Final exam (.pdf) *Accompanying Data File (.xlsx)
Dynamic Light Scattering (Legacy Document) (.doc)
(Practice data for Laplace Inversion: Milk or Dow Polystyrene 1683)
DLS Alignment (.pdf)
Bock/Siano Microemulsion recipe (.pdf)
Light Scattering Intensity Measurements (.doc)
Zimm Plots
Download Zip File for Program GuiDe (.zip)
GuiDe Manual; the Zimm Plot info is in an Appendix (.doc)
Related J. Chem.Ed. article (Russo, Fong, Temyanko & Ricks, J.Chem.Ed. 1999, 76(11), 1534.
Learn about Distribution analysis for Size Distribution (External link @ softscientific.com)
Measuring the Size of Nanoparticles in Aqueous Media Using Batch-Mode Dynamic Light Scattering (.pdf)
NIST-NCL Joint Assay Protocol, PCC-1 Version 1.2 ( http://dx.doi.org/10.6028/NIST.SP.1200-6)
Guide for Dynamic Light Scattering (DLS) Sample Preparation (External link @ Brookhaven Instruments)
OPALL- Open Polymer Active Learning Laboratory at Georgia Tech
Malvern ZetaSizer Nano ZS and Bettersize Benano 180 Zeta Pro
Intrinsic Viscosity (.doc)
Using the Wells-Brookfield Viscometer (.doc) (also requires instrument manual (BrookfieldLVTDCP (.pdf)))
Overview Document (.doc)
(Practice data: Velocity (.htm) and Equilibrium(.txt))
(Step-by-step Instructions for Velocity Run) (.doc)
Links to Microscopy Resources (Protocols, Tutorials, Vendors, Books, etc)
List of BOOKS Related to Microscopy
Microscopy from the Very Beginning (Zeiss Copyright: see Dr. Cueto)
Photography Through the Microscope (Kodak Copyright: see Dr. Cueto)
CHROMATOGRAPHY (GPC/SEC)
Manuals, Tutorials, Papers, Articles, etc. (Password Protected)
Gel Permeation Chromatography (GPC) (.doc)
Gel Permeation Chromatography with Light Scattering (GPC/LS) (.doc) (.pdf version)
Practice Data (.zip)
BOOKS
List of BOOKS Related to General Chromatography
List of BOOKS Related to GPC (SEC)
SPECTROSCOPY (UV-Vis / FL / IR / Raman)
Manuals, Tutorials, Papers, Articles, etc. (Password Protected)
BOOKS
List of BOOKS Related to Spectroscopy
List of BOOKS Related to Fluorescence
List of BOOKS Related to Infrared and Raman
Anotop (Whatman (Cytiva)) filter membranes
Whatman Whatman-filtration-product-guide (.pdf)
Refractive Index of Polymers (Scientific Polymer Products, Inc website)
Finding Chemical & Materials Properties: by Material Type: Polymers (MIT Libraries Link)
PAL Scheduling (Please Note: New Scheduler as of 09/27/2021)
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